Download 12th INTERNATIONAL CERAMICS CONGRESS Proceedings of the 12 by Edited by Pietro VINCENZINI World Academy of Ceramics and PDF

By Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by Maurizio FERRARI CNR-IFN, Italy Mrityunjay SINGH NASA Glenn Research Center, USA

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Read or Download 12th INTERNATIONAL CERAMICS CONGRESS Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 PART J including: Symposium PDF

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Extra info for 12th INTERNATIONAL CERAMICS CONGRESS Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 PART J including: Symposium

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The distance between the two electrodes was fixed to 1 mm with a nonconductive spacer. 5 mM dicyclohexylcarbodiimide (DCC) solution. A positive potential was applied to the 2aminoethanethiol-modified gold substrate, while a negative potential was applied to the counter electrode. 10V of potential vas applied to the system for 20 minutes. After the deposition, the system was washed with ethanol and dried with nitrogen stream. 5ml of concentred gold nanoparticles solution were added to 1 ml of 5mM 2-aminoethanethiol solution in ethanol.

Figure 4: FT-IR spectra of the uncalcined fibers(a) and calcined fibers (b) Figure 5 shows the SEM micrographs of the electrospun composite fibers with different magnification, which shows that these randomly oriented fibers are cylindrical and have smooth and uniform surfaces. The individual fibers have high aspect ratios (length/ diameter of fibers). The diameters of these composites fibers change widely from 80 nm to 500nm. The average diameters is 26 12th INTERNATIONAL CERAMICS CONGRESS PART J 200nm and the length of the composite fibers could reach several millimiters.

9H2O) (980g aluminum nitrate/1 L water), NH4OH water solution (28wt%) and polyvinyl alcohol ([C2H4O]n; PVAl) solution (8 wt% in water) to increase the viscosity. The sol-gel procedure used to produce the pseudoboehmite is described in a previous paper [4,5]. Characterization methods for the pseudoboehmite X-rays powder diffraction. For the samples dried at 70o C/24 hour’s diffraction data were recorded with a Rigaku MultiFlex difractometer with a fixed monocromator. 02o, λCuKα at room temperature.

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